Synthesis, Crystal Structure, and Characterization of (Z)-2-(3-chlorophenyl)-N’-hydroxyacetamidine
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Original research
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The compound (Z)-2-(3-chlorophenyl)-N’-hydroxyacetamidine, (2) was synthesized and characterized by 1H NMR, FT-IR, TGA, UV-Visible Spectra, and elemental analysis. Its molecular structure was solved by single-crystal X-ray diffraction method. The title molecule, C8H9ClN2O is crystallized in the monoclinic crystal system with the space group P21/c and with unit cell parameters a = 8.7092(4) Å, b = 8.2370(4) Å, c = 12.5256(6) Å, β = 102.252(3)°, and Z = 4. The molecular and crystal structure of the title molecule is stabilized by an intramolecular interaction of the type N—HċċċO, and the intermolecular interactions of types N—HċċċN and O—HċċċN.

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Journal
Title
Molecular Crystals and Liquid Crystals
Publisher
Molecular Crystals and Liquid Crystals
Publisher Country
United Kingdom
Indexing
Thomson Reuters
Impact Factor
1.5
Publication Type
Prtinted only
Volume
606
Year
2015
Pages
189-198