Synthesis, Identification and NMR of New Transdichloro- piperazine bis(ether-phosphine)ruthenium(II) Complex
- Publication Type
- Original research
- Authors
- Mohammed Suleiman
- Mousa Al-Noaimi
- Belkheir Hammouti
- Smaail Radi
- Taibi Ben Hadda
- Ahmed Boshaala
- Ismail Warad
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1-hTrans-dichloro-piperazine-bis(ether-phosphine)ruthenium(II)
complex of general formula Cl2Ru(Ph2PCH2CH2OCH3)2(C4H10N2) 2 was made available in good yield through treating
equimolar amounts of O)2 complex 1 with piperazine as
co-ligand. The hemilability ring open reaction of ether-phosphine inÇCl2Ru(Pcomplex 1 to
prepare complex 2 was monitored by 31P-NMR. The structure of complex 2 was
confirmed by elemental analysis, IR, 31P-NMR
1H-NMR,13C-NMR, FAB-MS and UV-visible spectroscopy.
Journal
- Title
- Suleiman & al. / Mor. J. Chem. 1 N°2 (2013) 29-32
- Publisher
- --
- Publisher Country
- Palestine
- Publication Type
- Both (Printed and Online)
- Volume
- --
- Year
- 2013
- Pages
- --