Crystal structure of 3-(thiophen-2-yl)-5-p-tolyl-4,5- dihydro-1H-pyrazole-1-carbothioamide
نوع المنشور
بحث أصيل
المؤلفون
النص الكامل
تحميل

In the title compound, C15H15N3S2, the central pyrazole ring adopts a twisted
conformation on the –CH—CH2– bond. Its mean plane makes dihedral angles of
7.19 (12) and 71.13 (11) with those of the thiophene and toluene rings,
respectively. The carbothiamide group [C( S)—N] is inclined to the pyrazole
ring mean plane by 16.8 (2). In the crystal, molecules are linked by N—H  S
hydrogen bonds, forming chains propagating along [010]. Within the chains,
there are N—H   interactions present. Between the chains there are weak
parallel slipped – interactions involving inversion-related thiophene and
pyrazole rings [inter-centroid distance = 3.7516 (14) A ° ; inter-planar distance =
3.5987 (10) A ° ; slippage = 1.06 A ° ].

المجلة
العنوان
Acta Crystallographica Section E
الناشر
Crystallographic Communications
بلد الناشر
المملكة المتحدة
Indexing
Scopus
معامل التأثير
None
نوع المنشور
Both (Printed and Online)
المجلد
71
السنة
2015
الصفحات
763-765