The title compound, C₁₆H₁₃NS (3) was synthesized and characterized by ¹H nuclear magnetic resonance (NMR), mass spectra (MS), infrared (IR), thermogravimetric analysis, differential scanning calorimeter (DSC) and finally the structure is confirmed by single crystal X-ray diffraction method. The compound 3 crystallizes in the monoclinic crystal system and space group C2/c, with crystal parameters, a = 10.99364(4) Å, b = 12.3517(3) Å, c = 20.1045(6) Å, β = 103.082(3)⁰, Z = 8, and V = 2647.30(14) ų. The structure of the compound reveals that the intermolecular interactions of the type C–H…π, C– H…N, and S…S. The packing diagram of the molecules in the unit cell exhibit three-dimensional architecture. In addition inter contacts involved in intermolecular interactions are quantified using Hirshfeld surfaces analysis.

العنوان

Molecular Crystals and Liquid Crystals

الناشر

Molecular Crystals and Liquid Crystals

بلد الناشر

المملكة المتحدة

Indexing

Thomson Reuters

معامل التأثير

1,5

نوع المنشور

مطبوع فقط

المجلد

609

السنة

2015

الصفحات

140-154